Code of Federal Regulations Title 40. Protection of Environment § 40.761.253 Chemical analysis

(a) Extract PCBs from the standard wipe sample collection medium and clean-up the extracted PCBs in accordance with either Method 3500B/3540C or Method 3500B/3550B from EPA's SW–846, Test Methods for Evaluating Solid Waste, or a method validated under subpart Q of this part. Use Method 8082 from SW–846, or a method validated under subpart Q of this part, to analyze these extracts for PCBs.

(b) Report all PCB sample concentrations in μg/100 cm² (16 square inches) of surface sampled. If sampling an area smaller than 100 cm², report converted sample concentrations in accordance with § 761.243(b).